Labsolar-6A 全玻璃自动在线微量气体分析系统

Labsolar-6a All-glass automatic on-line trace gas analysis system

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Labsolar-6A 全玻璃自动在线微量气体分析系统集成控制程序，操作简单方便，强大的兼容性，可通过更换不同的反应器实现光催化、光热催化、电催化、PEC光电化学等反应的微量气体检测。

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产品介绍
应用领域
文献
技术维护

关键特征

● 玻璃阀+自动执行器，实现气密性与效率兼顾的目标；

● 高效气体循环，既有效促进反应与催化剂之间的传质作用，又有效避免因产物分子的重吸附作用引发的副反应和逆反应，准确呈现催化剂的本征活性；

● 气体快速混合，气体混匀时间<10 min，确保产物检测的准确性；

● 集成控制程序，操作简单方便，准确性达科学级水准；

● 强大的兼容性，可通过更换不同的反应器实现光催化、光热催化、电催化、PEC光电化学等反应的微量气体检测。

应用领域

▲特别适用 ●较为适用 ○可以使用

▲ 光催化/光电催化分解水制氢/氧

▲ 光催化/光电催化全分解水

▲ 光催化/光电催化CO₂还原

▲ 光催化量子效率测量

▲ 光热催化（负压常压体系）

▲ 电催化HER、OER、CO₂RR

可搭配多种反应器拓展应用

气体循环参数

●气体混匀时间：H₂、O₂、CH₄、CO混匀时间<10 min；

●标准曲线线性：H₂含量为100 μL~10 mL范围时，R²>0.9995;

●重复性：同一浓度连续四次进样，RSD<3%;

●排气量：6 mL/次，负压至常压均能提供优异的循环驱动力;

●无源磁驱柱塞泵：管路中无电线接入，无氢爆风险，不产生电解水析氢干扰；具有单向阀结构，可实现所有管路的单向循环;

●取样方式：定量环位于多通玻璃取样阀，非色谱取样;

●循环管路:最窄管路为内径为3 mm，非小口径色谱管路，气体阻力小

外观结构参数

●反应器:可适配光催化反应器、光电催化、光热催化反应器;可根据实际实验需求定制;

●整机尺寸/mm:490 (L)×520 (W)×740 (H)

●金属防护箱体:对辐射可能的气体泄漏有一定防护作用

●光防护罩:便携式光防护罩，可有效防止光污染

系统管路参数

●绝压真空度:≤1.5 kPa

●使用压力范围:0 kPa~常压

●阀门数量:7

●管路体积:65 mL，系统富集能力强

●管路材质:高硼硅玻璃，高化学惰性，无吸附

●阀门工艺：高硼硅玻璃材质，阀塞与阀套采用对磨精磨工艺

●真空脂：进口道康宁真空脂，耐化学品的侵蚀，低蒸汽压力，低挥发性，工作温度：-40℃~200℃

●定量环：0.6 mL、2 mL可选，系统灵敏度可调

●储气瓶：150 mL，适用系统扩容和反应气如二氧化碳的存储

●管路控温：循环管路及进样管路均可进行控温，最高可控200℃ ；10段程序控温，控温精度±0.1℃；

●冷凝管（球形/蛇形）：冷凝充分，避免水蒸气进入气相色谱仪和真空泵

●冷阱（选配）：分离低沸点组分，延长真空泵使用寿命，提高系统真空度

控制单元参数

●软件模块：32位控制软件和4.5寸TFF彩色触摸屏；内置仪器方法用于控制玻璃阀动作、气相色谱仪及真空泵启停，操作简单；自动控制模式下，可实时显示阀门位置，具有安全防护预警功能；传感器自动提示更换真空脂；具有二级加密调试程序，用于设备调试、内部方法设定及资深用户灵活使用；实时显示系统内部反应压力、环境温度等参数；

●自动取样阀：高硼硅玻璃材质，内置定量环；多通复合取样阀，减少系统循环体积；支持手动、自动、半自动操作模式；

●真空泵：系统控制软件自动控制启停，间歇式工作，噪音小；含单向电磁阀，可防止泵油倒吸；

检测参数

●检测范围：H₂、O₂、CH₄、CO等多种微量气体；

●检出限/μmol：H₂：0.05；O₂：0.1；CH₄/CO：0.0005。

代表文献

华东理工大学李春忠团队引用Labsolar-6A光催化反应系统

青岛科技大学李镇江团队引用Labsolar-6A光催化反应系统.png

陕西师范大学蒋加兴团队引用Labsolar-6A光催化反应系统

陕西师范大学刘生忠团队引用Labsolar-6A光催化反应系统

应化所王颖团队引用Labsolar-6A光催化反应系统

深圳大学团队引用Labsolar-6A全玻璃微量气体分析系统.png

膜光催化
光降解气体污染物
光热催化（负压常压体系）
PEC光电化学
光催化量子效率测量
电化学
光催化二氧化碳还原
光催化全分解水
光催化分解水制氢/氧

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光解水water-splitting reaction